Hydrochloric Acid → Phenethylamine, alpha,alpha-dimethyl-4-dimethylamino-, dihydrochloride
반응식
[CH3:1][C:2]([NH:14]C(=O)C)([CH3:13])[CH2:3][C:4]1[CH:9]=[CH:8][C:7]([N:10]([CH3:12])[CH3:11])=[CH:6][CH:5]=1.[ClH:18]>O>[ClH:18].[ClH:18].[CH3:12][N:10]([CH3:11])[C:7]1[CH:8]=[CH:9][C:4]([CH2:3][C:2]([NH2:14])([CH3:13])[CH3:1])=[CH:5][CH:6]=1참가 물질
4
실험 절차
A solution of 3.5 of N-[α, α-dimethyl-β-(4-dimethylaminophenyl) ethyl]acetamide in a mixture of 25 ml of water and 25 ml of concentrated hydrochloric acid is reluxed for 16 hours. The solution is then evaporated under reduced pressure and the residue is recrystallized twice from methanol isopropyl ether. Yield: 1.1 g, m.p. 239,5°-240,5°.
후처리
- customThe solution is then evaporated under reduced pressure
- customthe residue is recrystallized twice from methanol isopropyl ether
출처 및 근거
- ORD 기록
- ord-b1f78afda1d940c9a3edc7cd831de829
- 출처 데이터셋
- uspto-grants-1976_12
- 특허 번호
- US03996381
반응 노트
불러오는 중…