2-(4-Chloroanilino)quinolizin-5-ium bromide → HCID 12446537, 화합물

HRID 1973386노트

반응식

HRID 1973386 반응식
[Br-].[Cl:2][C:3]1[CH:19]=[CH:18][C:6]([NH:7][C:8]2[CH:17]=[CH:16][N+:15]3[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=3)[CH:9]=2)=[CH:5][CH:4]=1>[OH-].[Na+]>[Cl:2][C:3]1[CH:4]=[CH:5][C:6]([N:7]=[C:8]2[CH:17]=[CH:16][N:15]3[C:10]([CH:11]=[CH:12][CH:13]=[CH:14]3)=[CH:9]2)=[CH:18][CH:19]=1

참가 물질

3

반응물 1

HCID 124465272-(4-Chloroanilino)quinolizin-5-ium bromide

생성물 1

HCID 12446537HCID 12446537, 화합물

시약·촉매·용매 1

HCID 14798Sodium Hydroxide용매

실험 절차

A suspension of 2-(4-chloroanilino)quinolizinium bromide (30 g., 0.09 mole) in 500 ml of 1N NaOH solution was warmed to 50° and stirred for 30 minutes. The crude product was removed by filtration and dried. The product (20 g., 87%) was recrystallized from ethanol to give material which melted at 183°-184°.

후처리

  1. temperaturewas warmed to 50°
  2. customThe crude product was removed by filtration
  3. customdried
  4. customThe product (20 g., 87%) was recrystallized from ethanol
  5. customto give material which melted at 183°-184°

출처 및 근거

ORD 기록
ord-f401ada7aa924e868d07d4af5354a9d0
출처 데이터셋
uspto-grants-1976_12
특허 번호
US03997547

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