Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-Toluenesulfonyl isocyanate → 5-sec.-BUTYL-2-(N-p-TOLUENESULFONYLCARBAMOYL)-1,3-CYCLOHEXANEDIONE
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-Toluenesulfonyl isocyanate | HCID 77703 | — |
| 반응물 | 5-(Butan-2-yl)cyclohexane-1,3-dione | HCID 20325617 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 5-sec.-BUTYL-2-(N-p-TOLUENESULFONYLCARBAMOYL)-1,3-CYCLOHEXANEDIONE | HCID 20325621 | — |
반응 단계
Reaction of equimolar amounts of 5-sec.-butyl-1,3-cyclohexanedione with p-toluenesulfonylisocyanate in benzene according to the procedure of Example 1 affords 5-sec.-BUTYL-2-(N-p-TOLUENESULFONYLCARBAMOYL)-1,3-CYCLOHEXANEDIONE, m.p. 92°-93° C. (corr.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03998879 |
| 출처 데이터셋 | uspto-grants-1976_12 |
| ORD ID | ord-7baf7702d08d41cfa54342a1fc595719 |
| 출처 메모 | uspto-grants-1976_12 |