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HRID1973763

反应详情

EQUATION

反应方程式

HRID 1973763 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(S(=O)(=O)N=C=O)cc1
HCID77703

p-Toluenesulphonyl isocyanate

C8H7NO3S

结构：CCC(C)C1CC(=O)CC(=O)C1
HCID20325617

5-(Butan-2-yl)cyclohexane-1,3-dione

C10H16O2

PRODUCTS

生成物

1
结构：CCC(C)C1CC(=O)C(C(=O)NS(=O)(=O)c2ccc(C)cc2)C(=O)C1
HCID20325621

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccccc1
溶剂HCID241

Benzene

C6H6

PROCEDURE

实验过程

Reaction of equimolar amounts of 5-sec.-butyl-1,3-cyclohexanedione with p-toluenesulfonylisocyanate in benzene according to the procedure of Example 1 affords 5-sec.-BUTYL-2-(N-p-TOLUENESULFONYLCARBAMOYL)-1,3-CYCLOHEXANEDIONE, m.p. 92°-93° C. (corr.).