Methyl iodide → HCID 20560070, 화합물

HRID 1974085노트

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HRID 1974085 반응식
[CH:1]([NH:3][C:4]1[CH:17]=[CH:16][CH:15]=[CH:14][C:5]=1[CH2:6][CH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][N:9]=1)=[O:2].C[I:19].[I-].[NH+]1C=CC=C[CH:22]=1>CC(C)=O>[I-:19].[CH:1]([NH:3][C:4]1[CH:17]=[CH:16][CH:15]=[CH:14][C:5]=1[CH2:6][CH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][N+:9]=1[CH3:22])=[O:2]

참가 물질

5

반응물 3

HCID 6328Methyl iodideHCID 20559958HCID 20559958, 화합물HCID 21863515PyridiuM iodide

생성물 1

HCID 20560070HCID 20560070, 화합물

시약·촉매·용매 1

HCID 180Acetone용매

반응 조건

온도
5 °C

실험 절차

A solution of 2-(o-formamidophenethyl)pyridine (55 g., 0.243 mole) and methyl iodide (38 g., 0.268 mole) in 500 ml. of acetone is refluxed for 20 hours. The mixture is cooled at 5° C. and filtered to provide 82 g. (92%) of the pyridinium iodide having melting point of 199.5°-201.5° C.

후처리

  1. filtrationfiltered
  2. customto provide 82 g

출처 및 근거

ORD 기록
ord-cc4efc4fb9ff41a18c02a1145f7e179d
출처 데이터셋
uspto-grants-1976_12
특허 번호
US04000143

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