Hydrochloric Acid → 2',4',6'-Triiodo-3'-ethyl-3-nitrobiphenyl-4-carboxylic acid

HRID 1976506노트

반응식

HRID 1976506 반응식
[I:1][C:2]1[C:7]([C:8](=O)[CH3:9])=[C:6]([I:11])[CH:5]=[C:4]([I:12])[C:3]=1[C:13]1[CH:18]=[CH:17][C:16]([C:19]([OH:21])=[O:20])=[C:15]([N+:22]([O-:24])=[O:23])[CH:14]=1.Cl>>[I:1][C:2]1[C:7]([CH2:8][CH3:9])=[C:6]([I:11])[CH:5]=[C:4]([I:12])[C:3]=1[C:13]1[CH:18]=[CH:17][C:16]([C:19]([OH:21])=[O:20])=[C:15]([N+:22]([O-:24])=[O:23])[CH:14]=1

참가 물질

3

반응물 2

HCID 313Hydrochloric AcidHCID 223419962',4',6'-Triiodo-3'-acetyl-3-nitrobiphenyl-4-carboxylic acid

생성물 1

HCID 223419932',4',6'-Triiodo-3'-ethyl-3-nitrobiphenyl-4-carboxylic acid

실험 절차

2′,4′,6′-triiodo-3′-acetyl-3-nitrobiphenyl-4-carboxylic acid (12) is then reacted with a zinc mercury amalgam and hydrochloric acid and heated to yield 2′,4′,6′-triiodo-3′-ethyl-3-nitrobiphenyl-4-carboxylic acid (13).

후처리

  1. temperatureheated

출처 및 근거

ORD 기록
ord-eb7372178bea48b68154be767e6ba1ca
출처 데이터셋
uspto-grants-2001_05
특허 번호
US06226352B1

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