Methyl bromoacetate → HCID 10839919, 화합물

HRID 1977338노트

반응식

[CH2:1]([C:8]1[S:12][C:11]2[CH:13]=[CH:14][CH:15]=[CH:16][C:10]=2[C:9]=1[C:17]1[CH:22]=[CH:21][C:20]([C:23]2[CH:28]=[CH:27][C:26]([OH:29])=[C:25]([Br:30])[CH:24]=2)=[CH:19][CH:18]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Br[CH2:32][C:33]([O:35]C)=[O:34]>>[CH2:1]([C:8]1[S:12][C:11]2[CH:13]=[CH:14][CH:15]=[CH:16][C:10]=2[C:9]=1[C:17]1[CH:22]=[CH:21][C:20]([C:23]2[CH:28]=[CH:27][C:26]([O:29][CH2:32][C:33]([OH:35])=[O:34])=[C:25]([Br:30])[CH:24]=2)=[CH:19][CH:18]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

참가 물질

반응물 2

HCID 60984Methyl bromoacetate

HCID 10790583HCID 10790583, 화합물

생성물 1

HCID 10839919HCID 10839919, 화합물

실험 절차

The title compound was prepared from 4′-(2-benzyl-benzo[b]thiophen-3-yl)-3-bromo-biphenyl-4-ol, and methyl bromoacetate, in substantially the same manner, as described in Example 2 step g , and was obtained as a white solid, mp 150-152° C.; MS m/e 528 (M+);

후처리

customwas obtained as a white solid, mp 150-152° C.

출처 및 근거

ORD 기록: ord-377b380f622543459cbc8bc0209bf6bc
출처 데이터셋: uspto-grants-2001_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06232322B1

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