Hydrochloric Acid → HCID 70247330, 화합물

HRID 1978418노트

반응식

HRID 1978418 반응식
C(OC([N:8]1[CH2:13][CH2:12][CH:11]([CH2:14][NH:15][C:16](=[O:31])[CH:17]=[CH:18][C:19]2[S:29][C:28]3[N:30]4[C:21](=[CH:22][N:23]=[C:24]4[CH:25]=[CH:26][CH:27]=3)[CH:20]=2)[CH2:10][CH2:9]1)=O)(C)(C)C.[ClH:32]>C(O)C>[ClH:32].[ClH:32].[NH:8]1[CH2:13][CH2:12][CH:11]([CH2:14][NH:15][C:16](=[O:31])[CH:17]=[CH:18][C:19]2[S:29][C:28]3[N:30]4[C:21](=[CH:22][N:23]=[C:24]4[CH:25]=[CH:26][CH:27]=3)[CH:20]=2)[CH2:10][CH2:9]1

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 70248359HCID 70248359, 화합물

생성물 1

HCID 70247330HCID 70247330, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

To this crude N-[1-(tert-butoxycarbonyl)piperidin-4-ylmethyl]-3-(5-thia-1,8b-diazaacenaphthylen-4-yl)acrylamide was added 1 ml of concentrated hydrochloric acid and the mixture was stirred at room temperature for 0.5 hour. After addition of ethanol, the mixture was stirred and the resulting precipitate was collected and washed serially with ethanol and diethyl ether to provide the title compound.

후처리

  1. stirringthe mixture was stirred
  2. customthe resulting precipitate was collected
  3. washwashed serially with ethanol and diethyl ether

출처 및 근거

ORD 기록
ord-373810fc5d264c3893955c649536d98b
출처 데이터셋
uspto-grants-2001_05
특허 번호
US06235731B1

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