Hydrochloric Acid → HCID 21994007, 화합물

HRID 1978496노트

반응식

HRID 1978496 반응식
C(OC([N:8]1[CH2:13][CH2:12][CH:11]([CH2:14][CH2:15][C:16](=[O:31])/[CH:17]=[CH:18]/[C:19]2[S:29][C:28]3[N:30]4[C:21](=[CH:22][N:23]=[C:24]4[CH:25]=[CH:26][CH:27]=3)[CH:20]=2)[CH2:10][CH2:9]1)=O)(C)(C)C.[ClH:32]>C(O)C>[ClH:32].[ClH:32].[NH:8]1[CH2:13][CH2:12][CH:11]([CH2:14][CH2:15][C:16](=[O:31])/[CH:17]=[CH:18]/[C:19]2[S:29][C:28]3[N:30]4[C:21](=[CH:22][N:23]=[C:24]4[CH:25]=[CH:26][CH:27]=3)[CH:20]=2)[CH2:10][CH2:9]1

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 21993956HCID 21993956, 화합물

생성물 1

HCID 21994007HCID 21994007, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

To the above crude (E)-5-[1-(tert-butoxycarbonyl)-piperidin-4-yl]-1-(5-thia-1,8b-diazaacenaphthylen-4-yl)-1-penten-3-one was added 5 ml of concentrated hydrochloric acid and the mixture was stirred at room temperature for 15 minutes. To this reaction mixture was added ethanol, followed by stirring, and the resulting precipitate was recovered by filtration and rinsed serially with ethanol and diethyl ether to provide the title compound.

후처리

  1. stirringby stirring
  2. filtrationthe resulting precipitate was recovered by filtration
  3. washrinsed serially with ethanol and diethyl ether

출처 및 근거

ORD 기록
ord-b8d82418373b46a2af9812f860e7a1a3
출처 데이터셋
uspto-grants-2001_05
특허 번호
US06235731B1

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