Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
O-Allylhydroxylamine → 2-[1-(Allyloxyimino)propyl]-5-(4-methanesulfonamidophenyl)-3-hydroxy-2-cyclohexen-1-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | O-Allylhydroxylamine | HCID 420841 | — |
| 반응물 | HCID 178458872 | HCID 178458872 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 2-[1-(Allyloxyimino)propyl]-5-(4-methanesulfonamidophenyl)-3-hydroxy-2-cyclohexen-1-one | HCID 136199969 | 68.8% |
반응 단계
Into 10 ml of tetrahydrofuran was dissolved 1.0 g of 5-(4-methanesulfonamidophenyl)-3-hydroxy-2-propionyl-2-cyclohexen-1-one and to the solution was added 0.5 g of allyloxyamine. The mixture was kept at room temperature for 15 hours and then it was treated with similar process in Example 1. Thus, 0.8 g of the objective compound was obtained. It was colorless crystals having a melting point of 134°-135° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04482740 |
| 출처 데이터셋 | uspto-grants-1984_11 |
| ORD ID | ord-7c91ec55f3d14d1481e47f800440632f |
| 출처 메모 | uspto-grants-1984_11 |