Dimethylformamide → N,N,N,2,2-Pentamethylpropan-1-aminium iodide

반응식

[CH2:1](N)[C:2](C)([CH3:4])[CH3:3].[CH2:7](N(CCCC)CCCC)CCC.C[I:21].[CH3:22][N:23]([CH:25]=O)[CH3:24]>>[I-:21].[CH3:22][N+:23]([CH2:25][C:2]([CH3:4])([CH3:3])[CH3:1])([CH3:7])[CH3:24]

참가 물질

반응물 4

HCID 6228Dimethylformamide

HCID 6328Methyl iodide

HCID 7622Tributylamine

HCID 79882Neopentylamine

생성물 1

HCID 13652289N,N,N,2,2-Pentamethylpropan-1-aminium iodide

실험 절차

11.51 Grams of neopentylamine (Aldrich), 48.7 grams of tributyl amine and 100 ml of DMF were mixed and cooled. 56 Grams of methyl iodide (Aldrich) were added dropwise and the reaction as carried out and worked up as in Example 1.

후처리

temperaturecooled
customthe reaction

출처 및 근거

ORD 기록: ord-b24055098b804e3ea5487e19d09e7b90
출처 데이터셋: uspto-grants-1985_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04510256

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