Methylhydrazine → (Aminomethylamino)((4-chlorophenyl)amino)methane-1-thione
반응식
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]=[C:9]=[S:10])=[CH:4][CH:3]=1.[CH3:11][NH:12][NH2:13]>C(O)C>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:9]([N:12]([CH3:11])[NH2:13])=[S:10])=[CH:4][CH:3]=1참가 물질
4
실험 절차
A mixture of 4-chlorophenylisothiocyanate (17.0 g, 0.10 mole) and methylhydrazine (5.0 g, 0.11 mole) in 80 ml of ethanol was stirred at room temperature for two hours. The reaction mixture was filtered to collect colorless crystalline N-(4-chlorophenyl)-1-methylhydrazinecarbothioamide (18.4 g, mp 152°-154° C.).
후처리
- filtrationThe reaction mixture was filtered
- customto collect colorless crystalline N-(4-chlorophenyl)-1-methylhydrazinecarbothioamide (18.4 g, mp 152°-154° C.)
출처 및 근거
- ORD 기록
- ord-6d4d2704efcb46fc958055c8e078625f
- 출처 데이터셋
- uspto-grants-1985_04
- 특허 번호
- US04514419
반응 노트
불러오는 중…