Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl 2-iodopropanoate → 6-t-Butoxycarbonylamino-4-N-(1-carbomethoxyethyl)-perhydro-1,4-thiazepin-5-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl 2-iodopropanoate | HCID 143426 | — |
| 반응물 | (Hexahydro-5-oxo-1,4-thiazepin-6-yl)carbamic acid, (1,1-dimethylethyl) ester | HCID 15591256 | — |
| 생성물 | 6-t-Butoxycarbonylamino-4-N-(1-carbomethoxyethyl)-perhydro-1,4-thiazepin-5-one | HCID 23318043 | 81.5% |
반응 단계
The above-named compound is prepared from 6-t-butoxycarbonylamino-perhydro-1,4-thiazepin-5-one (0.1 g) and methyl iodopropionate (0.11 g) according to the procedure described in Example 4. The product (0.11 g) is obtained after chromatography. The NMR spectrum is consistent with the assigned structure.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04594341 |
| 출처 데이터셋 | uspto-grants-1986_06 |
| ORD ID | ord-46d0b1599906477e95e6886d9c3ce496 |
| 출처 메모 | uspto-grants-1986_06 |