Phosphorus sulfide (P2S5) → HCID 20487524, 화합물

HRID 1995722노트

반응식

HRID 1995722 반응식
[CH2:1]([C:3]1[NH:4][C:5](=[S:18])[NH:6][C:7]=1[C:8](=O)[C:9]1[CH:14]=[CH:13][C:12]([F:15])=[C:11]([F:16])[CH:10]=1)[CH3:2].P12(SP3(SP(SP(S3)(S1)=S)(=S)S2)=S)=[S:20]>C1(C)C=CC=CC=1>[CH2:1]([C:3]1[NH:4][C:5](=[S:18])[NH:6][C:7]=1[C:8](=[S:20])[C:9]1[CH:14]=[CH:13][C:12]([F:15])=[C:11]([F:16])[CH:10]=1)[CH3:2]

참가 물질

4

반응물 2

HCID 14817Phosphorus sulfide (P2S5)HCID 20487469HCID 20487469, 화합물

생성물 1

HCID 20487524HCID 20487524, 화합물

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

Ten grams of 1,3-dihydro-4-ethyl-5-(3,4-difluorobenzoyl)-2H-imidazole-2-thione in toluene and phosphorus pentasulfide was heated at reflux temperature for 5 hours. Evaporation of the solvent provides the title compound.

후처리

  1. temperatureat reflux temperature for 5 hours
  2. customEvaporation of the solvent

출처 및 근거

ORD 기록
ord-1cfa91e2e95c4af68ca9588d8c4ee143
출처 데이터셋
uspto-grants-1983_09
특허 번호
US04405628

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