Hydrochloric Acid → methyl 1H-tetrazol-1-ylacetate

HRID 20268노트

반응식

HRID 20268 반응식
[N:1]1([CH2:6][C:7]([OH:9])=[O:8])[CH:5]=[N:4][N:3]=[N:2]1.Cl.O1CCOC[CH2:12]1>CO>[N:1]1([CH2:6][C:7]([O:9][CH3:12])=[O:8])[CH:5]=[N:4][N:3]=[N:2]1

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 312751,4-DioxaneHCID 5432071-Tetrazolylacetic acid

생성물 1

HCID 3153776methyl 1H-tetrazol-1-ylacetate

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

A mixture of tetrazol-1-yl acetic acid (5 g, 39 mmol) and 4M hydrochloric acid in dioxan (100 μL) in methanol (50 mL) was heated under reflux for 18 hours. The cooled mixture was evaporated under reduced pressure to provide the title compound.

후처리

  1. temperaturewas heated
  2. temperatureunder reflux for 18 hours
  3. customThe cooled mixture was evaporated under reduced pressure

출처 및 근거

ORD 기록
ord-2eec8cc3221c4243826d62a42e0801a2
출처 데이터셋
uspto-grants-2010_06
특허 번호
US07745630B2

반응 노트

불러오는 중…