Hydrochloric Acid → HCID 66905855, 화합물

HRID 2053206노트

반응식

HRID 2053206 반응식
[N+:1]([C:4]1[CH:5]=[C:6]([CH:14]=[CH:15][CH:16]=1)[CH:7]=[C:8]([CH2:12][CH3:13])[C:9]([OH:11])=[O:10])([O-:3])=[O:2].Cl.[CH3:18][CH2:19]O>>[CH2:18]([O:10][C:9](=[O:11])[C:8](=[CH:7][C:6]1[CH:14]=[CH:15][CH:16]=[C:4]([N+:1]([O-:3])=[O:2])[CH:5]=1)[CH2:12][CH3:13])[CH3:19]

참가 물질

4

반응물 3

HCID 313Hydrochloric AcidHCID 702EthanolHCID 990102-Ethyl-3-(3-nitrophenyl)propenoic acid

생성물 1

HCID 66905855HCID 66905855, 화합물

실험 절차

2-(3-Nitro-benzylidene)-butyric acid (500 mg, 2.27 mmol) was esterified by dissolving in EtOH (12.5 ml), adding conc HCl (0.25 ml) and heating to reflux for 8 h. The solvents were evaporated in vacuo to give the title compound.

후처리

  1. temperatureheating
  2. temperatureto reflux for 8 h
  3. customThe solvents were evaporated in vacuo

출처 및 근거

ORD 기록
ord-d168d43ed4544d86bbd2d8577d210644
출처 데이터셋
uspto-grants-2008_02
특허 번호
US07326732B2

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