Methanol → HCID 13625903, 화합물

반응식

Cl[C:2]1[CH:3]=[CH:4][C:5]([N+:16]([O-:18])=[O:17])=[C:6]([NH:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[CH3:15])[CH:7]=1.[Na].[CH3:20][OH:21]>>[CH3:20][O:21][C:2]1[CH:3]=[CH:4][C:5]([N+:16]([O-:18])=[O:17])=[C:6]([NH:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[CH3:15])[CH:7]=1

참가 물질

반응물 3

HCID 887Methanol

HCID 5360545Sodium

HCID 53269523HCID 53269523, 화합물

생성물 1

HCID 13625903HCID 13625903, 화합물

반응 조건

온도: 0 °C

실험 절차

1 g of 5-chloro-2-nitrophenyl-o-tolylamine was added to a solution of 1 g of sodium in 20 ml of methanol, and it was refluxed for 72 hours. Then, it is cooled to 0° C., and the crystalline product is suctioned off.

후처리

temperaturewas refluxed for 72 hours

출처 및 근거

ORD 기록: ord-bb296d42b5894f488b83023c3a34caa5
출처 데이터셋: uspto-grants-2008_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07329679B2

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