Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 1-Cyclooctylmethylimidazole hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 1-Cyclooctylmethylimidazole | HCID 20550238 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 1-Cyclooctylmethylimidazole hydrochloride | HCID 20550255 | — |
반응 단계
1-Cyclooctylmethylimidazole (~0.3 g) was dissolved in dry ether (30 ml), when a stream of dry hydrogen chloride was passed through the solution at -20° C. The resulting white precipitate was filtered off under dry nitrogen and recrystallised from ethyl acetate/petroleum ether (b.p. 40°-60° C.) to afford 1-cyclooctylmethylimidazole hydrochloride as a white solid, m.p. 20°-22° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04317830 |
| 출처 데이터셋 | uspto-grants-1982_03 |
| ORD ID | ord-5bdd3835cb974ba2bc4d7b9ee7b35fb0 |
| 출처 메모 | uspto-grants-1982_03 |