Benzylamine → 3-Benzylaminoacrylonitrile

HRID 2058790

반응식

HRID 2058790 반응식
[CH2:1]([NH2:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>C(O)C>[CH2:1]([NH:8][CH:3]=[CH:2][C:1]#[N:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

참가 물질

3

반응물 1

HCID 7504Benzylamine

생성물 1

HCID 705487013-Benzylaminoacrylonitrile수율 72.1%

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

9.7 g (0.1 mol) of 3-EAN and 21.4 g (0.2 mol) of benzylamine are refluxed for 4 h with removal of ethanol by distillation. Subsequent vacuum distillation yields 11.4 g of 3-benzylaminoacrylonitrile (72% with respect to 3-EAN).

후처리

  1. distillationSubsequent vacuum distillation

출처 및 근거

ORD 기록
ord-c179ea1549da4dd3b03926fca0d158d9
출처 데이터셋
uspto-grants-1982_03
특허 번호
US04319024

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