Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,6-Dichlorobenzoyl chloride → 2,6-Dichloro-N-(3-benzisoxazolyl)benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,6-Dichlorobenzoyl chloride | HCID 78392 | — |
| 반응물 | 1,2-Benzoxazol-3-amine | HCID 2779749 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 2,6-Dichloro-N-(3-benzisoxazolyl)benzamide | HCID 20546754 | — |
반응 단계
3-Aminobenzisoxazole (2 gram), 2,6-dichlorobenzoylchloride (2 gram), and 50 ml. of toluene are heated at reflux for 16 hours. After evaporation of the solvent at reduced pressure, the resultant oily semi-solid is triturated with ether. The solid so formed is then washed with ether and water and constitutes the desired product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04322429 |
| 출처 데이터셋 | uspto-grants-1982_03 |
| ORD ID | ord-4944d88c8d17409192df679111a9782c |
| 출처 메모 | uspto-grants-1982_03 |