4-Methoxybenzaldehyde → ethyl (E)-3-(4-methoxyphenyl)-2-methylprop-2-enoate
반응식
COc1ccc(C=O)cc1.CCOC(=O)C(C)C(=O)O>NCc1ccccc1.O=C(O)C(F)(F)F.CN(C)c1ccncc1.Cc1ccccc1>CCOC(=O)/C(C)=C/c1ccc(OC)cc1참가 물질
6
반응 조건
- 온도
- 50 °C
후처리
- temperatureThe product mixture was cooled to 25 °C.
- filtrationFiltered through a pad of celite · Organic 상 유지
- wash"The celite was washed with ethyl acetate (3 x 1 mL)."
- concentrationThe filtrate was concentrated under reduced pressure
- additionA 0.07 M stock solution of the internal standard ethylene carbonate (0.70 mL in CDCl3) was added.
출처 및 근거
- ORD 기록
- ord-f7814de4a6dc470c8fdac92d6e8f1243
- 출처 데이터셋
- Transfer learning optimization of 26 decarboxylative olefination reactions
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