1,2,3-Propanetricarboxylic acid → Tricarballylic acid tris(2-methylcyclohexylamide)
반응식
[CH2:1]([C:10]([OH:12])=O)[CH:2]([C:7]([OH:9])=O)[CH2:3][C:4]([OH:6])=O.[CH3:13][CH:14]1[CH2:19][CH2:18][CH2:17][CH2:16][CH:15]1[NH2:20]>C1(C)C(C)=CC=CC=1>[CH3:13][CH:14]1[CH2:19][CH2:18][CH2:17][CH2:16][CH:15]1[NH:20][C:4]([CH2:3][CH:2]([C:7]([NH:20][CH:15]1[CH2:16][CH2:17][CH2:18][CH2:19][CH:14]1[CH3:13])=[O:9])[CH2:1][C:10]([NH:20][CH:15]1[CH2:16][CH2:17][CH2:18][CH2:19][CH:14]1[CH3:13])=[O:12])=[O:6]참가 물질
4
실험 절차
Next, 3.52 g (20 mmol) of 1,2,3-propanetricarboxylic acid (made by Nacalai Tesque) and 13.6 g (120 mmol) of 2-methylcyclohexylamine were added to the xylene solution of a tricresol boric acid ester obtained above, and the contents were refluxed under heating and reacted for 3 hours. This gave a crude 1,2,3-propanetricarboxylic acid tris(2-methylcyclohexylamide) as a white solid.