Phenol → 2-Dodecylphenol

HRID 2068470

반응식

HRID 2068470 반응식
[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:8]=[CH:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]>>[CH2:19]([C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][C:1]=1[OH:7])[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][CH3:8]

참가 물질

3

반응물 2

HCID 996PhenolHCID 81831-Dodecene

생성물 1

HCID 1711442-Dodecylphenol수율 59.9%

실험 절차

First, dodecyl phenol was prepared. Specifically, to a 2-liter four-necked flask, 325 g of phenol and 30 g of dried activated clay (manufactured by MIZUSAWA INDUSTRIAL CHEMICALS, LTD.: product name, Galeonite #136) were added. 575 g of 1-dodecene was dropped in this mixture with agitation at 135 degrees C. for 4 hours. The activated clay was filtered, and then 537 g of dodecyl phenol was obtained by vacuum distillation.

후처리

  1. customFirst, dodecyl phenol was prepared
  2. filtrationThe activated clay was filtered

출처 및 근거

ORD 기록
ord-a47df7d20255403da9929f3bf66de330
출처 데이터셋
uspto-grants-2012_10
특허 번호
US08299004B2

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