Ethanol → HCID 70600924, 화합물
반응식
C([O:4][CH2:5][CH2:6][C:7]([C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)([OH:9])[CH3:8])(=O)C.[OH-].[Na+].C(O)C>O>[C:11]1([C:16]2[CH:17]=[CH:18][CH:19]=[CH:20][CH:21]=2)[CH:12]=[CH:13][CH:14]=[CH:15][C:10]=1[C:7]([OH:9])([CH3:8])[CH2:6][CH2:5][OH:4]참가 물질
5
실험 절차
A solution of 2.84 g. of 1-acetoxy-3-p-biphenylyl-3-butanol and 2 g. of NaOH in 30 ml. of 80% ethanol is boiled for 3 hours. Water is added and the mixture is extracted with chloroform and the extract is evaporated to give 3-p-biphenylyl-1,3-butanediol, m.p. 115- 117°.
후처리
- extractionthe mixture is extracted with chloroform
- customthe extract is evaporated
출처 및 근거
- ORD 기록
- ord-c62c3f64a9fa405cb70a18502799bd28
- 출처 데이터셋
- uspto-grants-1977_09
- 특허 번호
- US04049823
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