Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Amino-2,4-dibromoanthraquinone → 1-Amino-2-bromo-4-p-octadecylanilinoanthraquinone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Amino-2,4-dibromoanthraquinone | HCID 6681 | — |
| 반응물 | Potassium Acetate | HCID 517044 | — |
| 반응물 | 4-Octadecylaniline | HCID 3563365 | — |
| 촉매 | Cupric acetate | HCID 8895 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | 1-Amino-2-bromo-4-p-octadecylanilinoanthraquinone | HCID 21407064 | — |
반응 단계
A reactor was charged with 10 g of 1-amino-2,4-dibromoanthraquinone, 15 g of p-octadecyl-aniline, 20 g of pyridine, 0.2 g of copper acetate and 2.5 g of potassium acetate, and the reaction was effected at an elevated temperature of 115°-120° C. for 24 hours under stirring. A blue solid of 1-amino-2-bromo-4-p-octadecylanilinoanthraquinone was obtained by the reaction of the formula: ##STR9##
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04051052 |
| 출처 데이터셋 | uspto-grants-1977_09 |
| ORD ID | ord-b1f88d83b0ca4c7c80be16451e4aa1f3 |
| 출처 메모 | uspto-grants-1977_09 |