N-bromobutanimide → HCID 19858577, 화합물
반응식
C(=O)=O.CC(C)=O.[C:8]([S:12][C:13]1[CH:19]=[CH:18][C:16]([NH2:17])=[CH:15][CH:14]=1)([CH3:11])([CH3:10])[CH3:9].[Br:20]N1C(=O)CCC1=O>C(Cl)Cl>[C:8]([S:12][C:13]1[CH:14]=[CH:15][C:16]([NH2:17])=[C:18]([Br:20])[CH:19]=1)([CH3:11])([CH3:9])[CH3:10]참가 물질
5
실험 절차
To a cold (dry ice - acetone bath) stirred solution of 4-tert-butylthioaniline (25.6 g., 0.14 mole) in methylene chloride is added a slurry of N-bromosuccinimide (25.0 g., 0.14 mole) in methylene chloride in three equal portions. The reaction is allowed to come to room temperature with stirring overnight. The methylene chloride solution is washed with dilute aqueous sodium carbonate and water and then evaporated to give the desired product as a brown oil.
후처리
- customto come to room temperature
- washThe methylene chloride solution is washed with dilute aqueous sodium carbonate and water
- customevaporated
출처 및 근거
- ORD 기록
- ord-dcc08a60178d45f3a0ea7038e57a7b88
- 출처 데이터셋
- uspto-grants-1990_04
- 특허 번호
- US04913728
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