Thionyl Chloride → HCID 19860097, 화합물

HRID 2072666노트

반응식

HRID 2072666 반응식
[O:1]=[C:2]([N:9]1[CH2:18][CH2:17][C:16]2[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=2)[CH2:10]1)[CH2:3][N:4]([CH3:8])[CH2:5][CH2:6]O.S(Cl)([Cl:21])=O>C(Cl)(Cl)Cl>[Cl:21][CH2:6][CH2:5][N:4]([CH3:8])[CH2:3][C:2](=[O:1])[N:9]1[CH2:18][CH2:17][C:16]2[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=2)[CH2:10]1

참가 물질

4

반응물 2

HCID 24386Thionyl ChlorideHCID 14499658HCID 14499658, 화합물

생성물 1

HCID 19860097HCID 19860097, 화합물

시약·촉매·용매 1

HCID 6212Chloroform용매

실험 절차

The procedure is similar to that described in Example 6b), treating 5.6 g of 2-{N-[2-oxo-2-(1,2,3,4-tetrahydro-2-isoquinolyl) ethyl]methylamino}ethanol with an excess of thionyl chloride in chloroform.

출처 및 근거

ORD 기록
ord-c0b32e1c5dd844828b65a9ad4d959d10
출처 데이터셋
uspto-grants-1990_04
특허 번호
US04914092

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