홈MCP워크벤치Skills
홈워크벤치알림마이페이지
llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
  1. 홈
  2. /반응

Sodium Hydroxide → [1-(2-Diethylamino-ethyl)-2-(4-ethoxy-benzyl)-1H-benzoimidazol-5-yl]-thiourea

HRID 2074451
노트
인쇄 미리보기

반응식

HRID 2074451 반응식
[CH2:1]([N:3]([CH2:37][CH3:38])[CH2:4][CH2:5][N:6]1[C:10]2[CH:11]=[CH:12][C:13]([NH:15][C:16]([NH:18]C(=O)C3C=CC=CC=3)=[S:17])=[CH:14][C:9]=2[N:8]=[C:7]1[CH2:27][C:28]1[CH:33]=[CH:32][C:31]([O:34][CH2:35][CH3:36])=[CH:30][CH:29]=1)[CH3:2].[OH-].[Na+]>O1CCCC1.C(OCC)(=O)C>[CH2:37]([N:3]([CH2:1][CH3:2])[CH2:4][CH2:5][N:6]1[C:10]2[CH:11]=[CH:12][C:13]([NH:15][C:16]([NH2:18])=[S:17])=[CH:14][C:9]=2[N:8]=[C:7]1[CH2:27][C:28]1[CH:33]=[CH:32][C:31]([O:34][CH2:35][CH3:36])=[CH:30][CH:29]=1)[CH3:38]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

5

반응물 2

HCID 14798Sodium HydroxideHCID 16037889N-(1-(2-(diethylamino)ethyl)-2-(4-ethoxybenzyl)-1H-benzo[d]-imidazol-5-ylcarbamothioyl)benzamide

생성물 1

HCID 59799762[1-(2-Diethylamino-ethyl)-2-(4-ethoxy-benzyl)-1H-benzoimidazol-5-yl]-thiourea

시약·촉매·용매 2

HCID 8028Tetrahydrofuran용매HCID 8857Ethyl Acetate용매

실험 절차

N-(1-(2-(diethylamino)ethyl)-2-(4-ethoxybenzyl)-1H-benzo[d]-imidazol-5-ylcarbamothioyl)benzamide 20 (272 mg, 0.513 mmol) was dissolved in anhydrous tetrahydrofuran (10 mL) in a small, argon purged flask fitted with an condenser and magnetic stirbar. 2M NaOH (0.513 mL, 1.026 mmol) added and the solution was heated to reflux for 6 hours and cooled to room temperature overnight. The solution was concentrated and the residue was partitioned between H2O and ethyl acetate, transferred to a separatory funnel and the organic layer collected. The aqueous layer was further extracted with ethyl acetate and the combined organic layers were washed with brine (twice), dried over magnesium sulphate, filtered and concentrated to afford an off white solid which was slurried in hot ethyl acetate to yield white solid 21 [1-(2-Diethylamino-ethyl)-2-(4-ethoxy-benzyl)-1H-benzoimidazol-5-yl]-thiourea. Yield: 110 mg (50.3%). 1H NMR (DMSO) δ: 0.80 (t, 6H, J=7.1), 1.29 (t, 3H, J=7.0), 2.41 (q, 4H, J=7.0), 2.45-2.50 (m, 2H), 3.96 (q, 2H, J=6.9), 4.12 (t, 2H, J=6.7), 4.24 (s, 2H), 6.86 (d, 2H, J=8.6), 7.09 (dd, 1H, J=8.4, 1.5), 7.16 (d, 2H, J=8.7), 7.24 (br, 1-2H), 7.40 (d, 1H, J=8.5), 7.51 (s, 1H), 9.56 (s, 1H). MS (ESI): 426 (MH+, 100%)

후처리

  1. customfitted with an condenser
  2. temperaturethe solution was heated
  3. temperatureto reflux for 6 hours
  4. concentrationThe solution was concentrated
  5. customthe residue was partitioned between H2O and ethyl acetate
  6. customtransferred to a separatory funnel
  7. customthe organic layer collected
  8. extractionThe aqueous layer was further extracted with ethyl acetate
  9. washthe combined organic layers were washed with brine (twice),
  10. dry with materialdried over magnesium sulphate
  11. filtrationfiltered
  12. concentrationconcentrated
  13. customto afford an off white solid which

출처 및 근거

ORD 기록
ord-47149fda9958425fbcfdfac5e7cace93
출처 데이터셋
uspto-grants-2011_04
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US07919510B2

반응 노트

불러오는 중…

이 페이지에서참가 물질실험 절차후처리출처 및 근거반응 노트