Methyl Isocyanate → N-Methyl 3-(3-aminocarbonylphenoxy)-1-azetidinecarboxamide

반응식

[NH:1]1[CH2:4][CH:3]([O:5][C:6]2[CH:7]=[C:8]([CH:12]=[CH:13][CH:14]=2)[C:9]([NH2:11])=[O:10])[CH2:2]1.[CH3:15][N:16]=[C:17]=[O:18]>>[CH3:15][NH:16][C:17]([N:1]1[CH2:4][CH:3]([O:5][C:6]2[CH:14]=[CH:13][CH:12]=[C:8]([C:9]([NH2:11])=[O:10])[CH:7]=2)[CH2:2]1)=[O:18]

참가 물질

반응물 2

HCID 12228Methyl Isocyanate

HCID 128125073-(3-Azetidinyloxy)benzamide

생성물 1

HCID 13420168N-Methyl 3-(3-aminocarbonylphenoxy)-1-azetidinecarboxamide

실험 절차

The compound was prepared from 3-(3-azetidinyloxy) benzamide and methylisocyanate as described in Example 6 of U.S. Pat. No. 4,226,861, m.p. 238°-240° C.

출처 및 근거

ORD 기록: ord-98d845202d26433587b76c4db7dbbb27
출처 데이터셋: uspto-grants-1993_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05183902

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