Hydrazine → Tetradecanehydrazide

HRID 2081661

반응식

HRID 2081661 반응식
[NH2:1][NH2:2].[C:3]([O:18]C)(=O)[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]>CO>[C:3]([NH:1][NH2:2])(=[O:18])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

참가 물질

4

반응물 2

HCID 9321HydrazineHCID 31284Methyl Myristate

생성물 1

HCID 2748033Tetradecanehydrazide수율 43.9%

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Hydrazine (1.9 mL, 0.058 mol) was added to a solution of methyl tetradecanoate (13.96 g, 0.058 mol) in methanol (300 mL) and the solution refluxed for 3 days. The mixture was allowed to cool and filtered to yield 6.17 g of a crystalline solid, m.p. 107°-111° C.

후처리

  1. temperaturethe solution refluxed for 3 days
  2. temperatureto cool
  3. filtrationfiltered

출처 및 근거

ORD 기록
ord-afcf65b2ba08436fa2698374f5ed43d2
출처 데이터셋
uspto-grants-1993_02
특허 번호
US05185358

연결된 노트

불러오는 중…