Hydrochloric Acid → 2,4-Dichloro-6-methylbenzylamine hydrochloride

HRID 2099313노트

반응식

HRID 2099313 반응식
[Cl:1][C:2]1[CH:9]=[C:8]([Cl:10])[CH:7]=[C:6]([CH3:11])[C:3]=1[C:4]#[N:5].Cl>O1CCOCC1>[ClH:1].[Cl:1][C:2]1[CH:9]=[C:8]([Cl:10])[CH:7]=[C:6]([CH3:11])[C:3]=1[CH2:4][NH2:5]

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 28009652,4-Dichloro-6-methylbenzonitrile

생성물 1

HCID 467858042,4-Dichloro-6-methylbenzylamine hydrochloride

시약·촉매·용매 1

HCID 312751,4-Dioxane용매

실험 절차

The preparation takes place in analogy to Example 6A from 2,4-dichloro-6-methylbenzonitrile with subsequent treatment with 4N hydrochloric acid in dioxane.

출처 및 근거

ORD 기록
ord-138cfb41756f4ae0a67635a0072d0ffb
출처 데이터셋
uspto-grants-2009_08
특허 번호
US07569563B2

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