Benzenesulfonyl chloride → (1-Benzenesulfonyl-5-methoxy-1H-indol-3-yl)-acetic acid

HRID 2100447

반응식

[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:9](=[CH:10][CH:11]=1)[NH:8][CH:7]=[C:6]2[CH2:12][C:13]([OH:15])=[O:14].[C:16]1([S:22](Cl)(=[O:24])=[O:23])[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>>[C:16]1([S:22]([N:8]2[C:9]3[C:5](=[CH:4][C:3]([O:2][CH3:1])=[CH:11][CH:10]=3)[C:6]([CH2:12][C:13]([OH:15])=[O:14])=[CH:7]2)(=[O:24])=[O:23])[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1

참가 물질

반응물 2

HCID 7369Benzenesulfonyl chloride

HCID 189865-Methoxyindoleacetic acid

생성물 1

HCID 18450002(1-Benzenesulfonyl-5-methoxy-1H-indol-3-yl)-acetic acid

실험 절차

(1-Benzenesulfonyl-5-methoxy-1H-indol-3-yl)-acetic acid 100 was prepared from commercially available (5-methoxy-1H-indol-3-yl)-acetic acid and benzene sulfonyl chloride using the protocol as described in step 8, example 4. (M−1=344.4)

출처 및 근거

ORD 기록: ord-b9541173ce524210b6b6bd23f7f373b5
출처 데이터셋: uspto-grants-2009_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07572806B2

연결된 노트

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