Hydrochloric Acid → 4-(Ethyl-3-methylanilino)butyric acid
반응식
Cl.C([O:4][C:5](=[O:19])[CH2:6][CH2:7][CH2:8][N:9]([CH2:17][CH3:18])[C:10]1[CH:15]=[CH:14][CH:13]=[C:12]([CH3:16])[CH:11]=1)C>O1CCOCC1.O>[CH2:17]([N:9]([CH2:8][CH2:7][CH2:6][C:5]([OH:19])=[O:4])[C:10]1[CH:15]=[CH:14][CH:13]=[C:12]([CH3:16])[CH:11]=1)[CH3:18]참가 물질
5
반응 조건
- 온도
- 95 °C
실험 절차
4N Solution (100 ml) of hydrogen chloride in dioxane and water (20 ml) was added to the compound (14.1 g) obtained in Step 1, and the mixture was stirred at 95° C. for 12 hours. The solvent was evaporated to give the title compound (13.7 g).
후처리
- customThe solvent was evaporated
출처 및 근거
- ORD 기록
- ord-79ba79833c4742f094ebae627fd0d2db
- 출처 데이터셋
- uspto-grants-2009_08
- 특허 번호
- US07572815B2
반응 노트
불러오는 중…