1,4-Dichlorobenzene → HCID 14298267, 화합물

HRID 2105098노트

반응식

HRID 2105098 반응식
[CH3:1][C:2]1[S:3][C:4]2[CH:10]=[C:9]([N+:11]([O-:13])=[O:12])[CH:8]=[CH:7][C:5]=2[N:6]=1.[CH2:14]([I:16])[CH3:15].C1C(Cl)=CC=C(Cl)C=1>C(OCC)(=O)C>[I-:16].[CH2:14]([N+:6]1[C:5]2[CH:7]=[CH:8][C:9]([N+:11]([O-:13])=[O:12])=[CH:10][C:4]=2[S:3][C:2]=1[CH3:1])[CH3:15]

참가 물질

5

반응물 3

HCID 46851,4-DichlorobenzeneHCID 6340IodoethaneHCID 76250Benzothiazole, 2-methyl-6-nitro-

생성물 1

HCID 14298267HCID 14298267, 화합물

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

반응 조건

온도
120 °C

실험 절차

To 2-methyl-6-nitrobenzothiazole (0.36 g) was added ethyl iodide (1.5 ml) and dichlorobenzene (20 ml). The mixture was heated to 120° C. for 2 days and then allowed to cool to room temperature. Ethyl acetate was added and the resulting precipitate removed by filtration. Drying in a vacuum oven gave the desired material (80 mg).

후처리

  1. temperatureto cool to room temperature
  2. customthe resulting precipitate removed by filtration
  3. customDrying in a vacuum oven

출처 및 근거

ORD 기록
ord-579d121d2d62472e835a9521a51b51f6
출처 데이터셋
uspto-grants-2009_08
특허 번호
US07579140B2

반응 노트

불러오는 중…