Sodium Hydroxide → HCID 86613671, 화합물

HRID 2105632노트

반응식

HRID 2105632 반응식
[CH2:1]([C@H:7]1[CH2:11][CH:10]([CH3:12])[O:9][C:8]1=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].[OH-:14].[Na+:15]>C(O)C>[OH:9][CH:10]([CH3:12])[CH2:11][C@H:7]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH3:6])[C:8]([O-:13])=[O:14].[Na+:15]

참가 물질

4

반응물 2

HCID 14798Sodium HydroxideHCID 57809406(3S)-3-Hexyl-5-methyloxolan-2-one

생성물 1

HCID 86613671HCID 86613671, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

반응 조건

온도
75 °C

실험 절차

To an ethanol solution of the compound prepared in Example 1(6) was added an equivalent of an aqueous solution of sodium hydroxide, and the mixture was stirred at 75° C. for 3 hours. The reaction mixture was concentrated to give the compound of the present invention having the following physical data.

후처리

  1. concentrationThe reaction mixture was concentrated
  2. customto give the compound of the present invention

출처 및 근거

ORD 기록
ord-1516e44be0fa4d68829fa8e60baec042
출처 데이터셋
uspto-grants-2009_08
특허 번호
US07579375B2

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