Triethylamine → HCID 23047606, 화합물

HRID 2107264노트

반응식

HRID 2107264 반응식
[C:1]1([CH3:15])[C:2]([NH:7][C:8]2[S:9][CH:10]=[C:11]([CH2:13][OH:14])[N:12]=2)=[CH:3][CH:4]=[CH:5][CH:6]=1.C(N(CC)CC)C>CS(C)=O>[C:1]1([CH3:15])[C:2]([NH:7][C:8]2[S:9][CH:10]=[C:11]([CH:13]=[O:14])[N:12]=2)=[CH:3][CH:4]=[CH:5][CH:6]=1

참가 물질

4

반응물 2

HCID 8471TriethylamineHCID 16769476HCID 16769476, 화합물

생성물 1

HCID 23047606HCID 23047606, 화합물

시약·촉매·용매 1

HCID 679Dimethyl Sulfoxide용매

실험 절차

Following a procedure similar to that described in Preparation 44, the desired compound was prepared from 6.12 g of 2-(o-toluidino)thiazole-4-ylmethanol, 13.2 g of a sulfur trioxide pyridine complex, 12 ml of triethylamine and 210 ml of dimethyl sulfoxide, as pale brown prismatic crystals having the following physical properties.

후처리

  1. customthat described in Preparation 44

출처 및 근거

ORD 기록
ord-f4d5b64d9b4944fab3df556a8f2e963a
출처 데이터셋
uspto-grants-1990_06
특허 번호
US04933355

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