Ethyl bromopyruvate → Ethyl 2-[(prop-2-en-1-yl)amino]-1,3-thiazole-4-carboxylate

HRID 2107281

반응식

HRID 2107281 반응식
[CH2:1]([NH:4][C:5]([NH2:7])=[S:6])[CH:2]=[CH2:3].Br[CH2:9][C:10](=O)[C:11]([O:13][CH2:14][CH3:15])=[O:12]>C(O)C>[CH2:1]([NH:4][C:5]1[S:6][CH:9]=[C:10]([C:11]([O:13][CH2:14][CH3:15])=[O:12])[N:7]=1)[CH:2]=[CH2:3]

참가 물질

4

반응물 2

HCID 66144Ethyl bromopyruvateHCID 1549517Allylthiourea

생성물 1

HCID 7171906Ethyl 2-[(prop-2-en-1-yl)amino]-1,3-thiazole-4-carboxylate

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

The reaction described in Preparation 42 was repeated but using 20 g of allylthiourea, 37 g of ethyl bromopyruvate and 200 ml of ethanol, giving the title compound as a pale yellow powder.

후처리

  1. customThe reaction described in Preparation 42

출처 및 근거

ORD 기록
ord-0e9e1c5001ae40ca92cf91cc4ae3ef25
출처 데이터셋
uspto-grants-1990_06
특허 번호
US04933355

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