Ethyl 2-[(prop-2-en-1-yl)amino]-1,3-thiazole-4-carboxylate → HCID 15053559, 화합물

HRID 2107282

반응식

HRID 2107282 반응식
[CH2:1]([NH:4][C:5]1[S:6][CH:7]=[C:8]([C:10](OCC)=[O:11])[N:9]=1)[CH:2]=[CH2:3].[H-].[Al+3].[Li+].[H-].[H-].[H-]>O1CCCC1>[CH2:1]([NH:4][C:5]1[S:6][CH:7]=[C:8]([CH2:10][OH:11])[N:9]=1)[CH:2]=[CH2:3]

참가 물질

4

반응물 2

HCID 7171906Ethyl 2-[(prop-2-en-1-yl)amino]-1,3-thiazole-4-carboxylateHCID 21226445Aluminium lithium hydride

생성물 1

HCID 15053559HCID 15053559, 화합물

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

The reaction described in Preparation 15 was repeated, but using 10 g of ethyl 2-allylaminothiazole-4-carboxylate, 2.7 g of lithium aluminum hydride and 150 ml of tetrahydrofuran. giving the title compound as pale brown needles.

후처리

  1. customThe reaction described in Preparation 15

출처 및 근거

ORD 기록
ord-96b70246f9234f0a9c9bdb303be4c2c6
출처 데이터셋
uspto-grants-1990_06
특허 번호
US04933355

연결된 노트

불러오는 중…