Chloroform → HCID 22411936, 화합물
반응식
[C:1]1([C:7]2[NH:8][C:9]([CH3:17])=[C:10]([CH:12](O)[CH:13]([CH3:15])[CH3:14])[N:11]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C(Cl)(Cl)[Cl:19]>O=S(Cl)Cl>[ClH:19].[C:1]1([C:7]2[NH:8][C:9]([CH3:17])=[C:10]([CH:12]([Cl:19])[CH:13]([CH3:15])[CH3:14])[N:11]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1참가 물질
4
실험 절차
27 g of 2-phenyl-4-(1-hydroxy-2-methylpropyl)-5-methyl-1H-imidazole are dissolved in 700 ml of chloroform with 44 ml of SOCl2 and refluxed for 5 hours. 2-Phenyl-5-methyl-4-(1-chloro-2-methylpropyl)-1H-imidazole hydrochloride is isolated in quantitative yield.
후처리
- temperaturerefluxed for 5 hours
출처 및 근거
- ORD 기록
- ord-1f89aad97a584c0e9d3a3a777f5cdbe0
- 출처 데이터셋
- uspto-grants-1990_06
- 특허 번호
- US04935417
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