1-Chloro-2-(diethylamine)ethane hydrochloride → HCID 69065330, 화합물

HRID 2109022노트

반응식

HRID 2109022 반응식
[C:1]([NH:4][C:5]1[CH:10]=[CH:9][C:8]([S:11]([OH:13])=[O:12])=[CH:7][CH:6]=1)(=[O:3])[CH3:2].[OH-].[Na+].[CH3:16][CH2:17][N:18]([CH2:21][CH2:22]Cl)[CH2:19][CH3:20].Cl>O>[C:1]([NH:4][C:5]1[CH:6]=[CH:7][C:8]([S:11]([CH2:16][CH2:17][N:18]([CH2:21][CH3:22])[CH2:19][CH3:20])(=[O:13])=[O:12])=[CH:9][CH:10]=1)(=[O:3])[CH3:2]

참가 물질

5

반응물 3

HCID 133631-Chloro-2-(diethylamine)ethane hydrochlorideHCID 14798Sodium Hydroxide2회HCID 4121504-(Acetylamino)benzenesulfinic acid

생성물 1

HCID 69065330HCID 69065330, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

9.0 g of 4-acetamido-phenylsulphinic acid are dissolved in 10 ml of water and 45 ml of 1N sodium hydroxide solution and 9.47 g of 2-chlorotriethylamine hydrochloride are added. The mixture is stirred for 5 hours at reflux temperature. After cooling, sodium hydroxide solution is added until an alkaline reaction is obtained, the mixture is extracted with ethyl acetate, dried over magnesium sulphate and finally the solvent is eliminated.

후처리

  1. temperatureat reflux temperature
  2. temperatureAfter cooling
  3. customis obtained
  4. extractionthe mixture is extracted with ethyl acetate
  5. dry with materialdried over magnesium sulphate

출처 및 근거

ORD 기록
ord-d6396b351f864c0abea1e4bff9a0de9c
출처 데이터셋
uspto-grants-2009_04
특허 번호
US07514468B2

반응 노트

불러오는 중…