Hydrochloric Acid → 25442-63-1

HRID 2109023노트

반응식

HRID 2109023 반응식
C([NH:4][C:5]1[CH:10]=[CH:9][C:8]([S:11]([CH2:14][CH2:15][N:16]([CH2:19][CH3:20])[CH2:17][CH3:18])(=[O:13])=[O:12])=[CH:7][CH:6]=1)(=O)C.Cl>C(O)C>[CH2:19]([N:16]([CH2:17][CH3:18])[CH2:15][CH2:14][S:11]([C:8]1[CH:7]=[CH:6][C:5]([NH2:4])=[CH:10][CH:9]=1)(=[O:13])=[O:12])[CH3:20]

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 69065330HCID 69065330, 화합물

생성물 1

HCID 41421425442-63-1

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

9.85 g of N-acetyl-4-(2-diethylamino-ethyl-sulphonyl)-aniline (educt XVII) are dissolved in 25 ml of ethanol and 100 ml of 3N hydrochloric acid are added. The mixture is stirred for 1 hour at reflux temperature. After cooling it is neutralised, extracted three times with methylene chloride, dried over magnesium sulphate and finally the solvent is eliminated.

후처리

  1. temperatureat reflux temperature
  2. temperatureAfter cooling it
  3. extractionextracted three times with methylene chloride
  4. dry with materialdried over magnesium sulphate

출처 및 근거

ORD 기록
ord-f9ce0c221a7944b390771b1a679bba56
출처 데이터셋
uspto-grants-2009_04
특허 번호
US07514468B2

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