Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
tert-Butyl bromoacetate → 1,1-Dimethylethyl N-[4-cyano-3-(trifluoromethyl)phenyl]-N-(3,3,3-trifluoropropyl)glycinate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | tert-Butyl bromoacetate | HCID 79177 | — |
| 반응물 | 2-(Trifluoromethyl)-4-[(3,3,3-trifluoropropyl)amino]benzonitrile | HCID 57633757 | — |
| 생성물 | 1,1-Dimethylethyl N-[4-cyano-3-(trifluoromethyl)phenyl]-N-(3,3,3-trifluoropropyl)glycinate | HCID 11749814 | — |
반응 단계
Synthesized as described in example 1B using 2-(trifluoromethyl)-4-[(3,3,3-trifluoropropyl)amino]benzonitrile and tert-butyl bromoacetate: 1H NMR (400 MHz, CDCl3) δ 7.64 (d, J=8.8 Hz, 1H), 6.84 (d, J=2.6 Hz, 1H), 6.73 (dd, J=8.8, 2.6 Hz, 1H), 4.03 (s, 2H), 3.74 (t, J=7.5 Hz, 2H), 2.57-2.45 (m, 2H), 1.45 (s, 9H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07514470B2 |
| 출처 데이터셋 | uspto-grants-2009_04 |
| ORD ID | ord-c6d0a58330fe43459e0d13be789656cc |
| 출처 메모 | uspto-grants-2009_04 |