3-Iodophthalic acid → 3-Iodophthalic anhydride
반응식
[I:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:4]([C:5]([OH:7])=O)[C:3]=1[C:11]([OH:13])=[O:12]>C(O)(=O)C>[I:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:4]2[C:5]([O:13][C:11](=[O:12])[C:3]=12)=[O:7]참가 물질
3
반응 조건
- 온도
- 145 °C
실험 절차
3-Iodophthalic acid (4.00 g, 13.7 mmol) was dissolved in anhydrous acetic acid, and the solution was stirred at 145° C. for 1 hour. The solvent of the reaction mixture was evaporated under reduced pressure and the residue was purified by slurry using diisopropylether to obtain 3-iodophthalic acid anhydride (3.6 g, yield 96%).
후처리
- customThe solvent of the reaction mixture was evaporated under reduced pressure
- customthe residue was purified by slurry
출처 및 근거
- ORD 기록
- ord-2fc0ada1147d4bd8ade7960d2b1c0711
- 출처 데이터셋
- uspto-grants-2010_06
- 특허 번호
- US07745641B2
반응 노트
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