m-Chloroperbenzoic acid → 4-(4-Fluoro-phenyl)-pyridine 1-oxide

HRID 2113544노트

반응식

HRID 2113544 반응식
ClC1C=CC=C(C(OO)=[O:9])C=1.[F:12][C:13]1[CH:18]=[CH:17][C:16]([C:19]2[CH:24]=[CH:23][N:22]=[CH:21][CH:20]=2)=[CH:15][CH:14]=1>C(Cl)(Cl)Cl>[F:12][C:13]1[CH:14]=[CH:15][C:16]([C:19]2[CH:20]=[CH:21][N+:22]([O-:9])=[CH:23][CH:24]=2)=[CH:17][CH:18]=1

참가 물질

4

반응물 2

HCID 70297m-Chloroperbenzoic acidHCID 155443714-(4-Fluorophenyl)pyridine

생성물 1

HCID 187002504-(4-Fluoro-phenyl)-pyridine 1-oxide

시약·촉매·용매 1

HCID 6212Chloroform용매

반응 조건

온도
0 °C

실험 절차

3.5 g (10.2 mmol) of meta-chloroperbenzoic acid are added to a solution of 1.18 g (6.81 mmol) of 4-(4-fluorophenyl)pyridine in 5 mL of chloroform cooled to 0° C. The suspension is stirred for 30 minutes.

출처 및 근거

ORD 기록
ord-91873448255c456fb82bfc36d4f840d8
출처 데이터셋
uspto-grants-2008_10
특허 번호
US07432269B2

반응 노트

불러오는 중…