Phthalic Anhydride → Caprolactone acrylate

HRID 2118769

반응식

HRID 2118769 반응식
C1(=O)[O:6][C:4](=[O:5])[C:3]2=CC=CC=[C:2]12.[C:12]1(=[O:22])[O:17][C:15](=O)[CH:14]2[CH2:18][CH2:19][CH2:20]CC12>>[C:4]([OH:6])(=[O:5])[CH:3]=[CH2:2].[C:12]1(=[O:22])[O:17][CH2:15][CH2:14][CH2:18][CH2:19][CH2:20]1

참가 물질

3

반응물 2

HCID 6811Phthalic AnhydrideHCID 85689Hexahydrophthalic anhydride

생성물 1

HCID 66599592Caprolactone acrylate

반응 조건

온도
125 °C

실험 절차

An acid-terminated caprolactone acrylate was prepared by combining 37.0 g of phthalic anhydride, 19.25 g of hexahydrophthalic anhydride, and 129.0 g of TONE Monomer M-100 in a glass, four-neck reaction flask equipped with a stirrer, a thermometer, an air inlet and an air outlet, and heating them at 125° C. for 3.5 hours. The product was recovered and found to have an Acid Number of 114 and a viscosity of 1690 cp when measured at 25° C.

후처리

  1. customequipped with a stirrer
  2. customThe product was recovered
  3. custommeasured at 25° C.

출처 및 근거

ORD 기록
ord-9a4938125f1c4bea98acfbe799c2411e
출처 데이터셋
uspto-grants-1987_07
특허 번호
US04680361

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