Acetic Anhydride → 1-Acetyl-2-benzhydrylimino-1,3-diazacycloheptane

반응식

[CH:1]([N:14]=[C:15]1[NH:21][CH2:20][CH2:19][CH2:18][CH2:17][NH:16]1)([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:22](OC(=O)C)(=[O:24])[CH3:23]>>[C:22]([N:21]1[CH2:20][CH2:19][CH2:18][CH2:17][NH:16][C:15]1=[N:14][CH:1]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1)(=[O:24])[CH3:23]

참가 물질

반응물 2

HCID 7918Acetic Anhydride

HCID 178420335HCID 178420335, 화합물

생성물 1

HCID 1784738141-Acetyl-2-benzhydrylimino-1,3-diazacycloheptane

실험 절차

A mixture of 0.50 g of 2-benzhydrylimino-1,3-diazacycloheptane and 0.237 g of acetic anhydride was reacted in substantially the same procedure as in Example 40 to give 1-acetyl-2-benzhydrylimino-1,3-diazacycloheptane having a melting point of 250° to 252° C.

후처리

customwas reacted in substantially the same procedure as in Example 40

출처 및 근거

ORD 기록: ord-25f99f6948bf4537b1a02bcb0e0f54cc
출처 데이터셋: uspto-grants-1979_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04136188

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