Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetone → N-[4-(hexadecylamino)benzoyl]urea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetone | HCID 180 | — |
| 반응물 | 4-Hexadecylaminobenzoyl chloride hydrochloride | HCID 13255322 | — |
| 반응물 | Urea, monosodium salt | HCID 86736265 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | N-[4-(hexadecylamino)benzoyl]urea | HCID 20437348 | — |
반응 단계
The 12.6 g. of 4-(hexadecylamino)benzoyl chloride hydrochloride in methylene chloride is added to 5 g. of sodium urea in 30 ml. of acetone and the mixture is stirred at 20° C. for 18 hours. Dilute alkali is added and the solid washed with alkaline aqueous acetone. Recrystallization from ethanol gives pure white crystals of product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04136256 |
| 출처 데이터셋 | uspto-grants-1979_01 |
| ORD ID | ord-090e718136fa4ead865c59a0da671699 |
| 출처 메모 | uspto-grants-1979_01 |