반응식
C1(=O)NC(=O)C2=CC=CC=C12.NN.[CH3:14][N:15]=[C:16]=[S:17].[CH3:18][C:19]1[N:20]=[C:21]([S:24][CH2:25][CH2:26][CH2:27][NH:28]C(N)=S)[O:22][CH:23]=1>>[CH3:14][NH:15][C:16]([NH:28][CH2:27][CH2:26][CH2:25][S:24][C:21]1[O:22][CH:23]=[C:19]([CH3:18])[N:20]=1)=[S:17]참가 물질
5
실험 절차
Treatment of the phthalimide compound (3.0 g.) with hydrazine (1.53 g.) followed by reaction of the product directly with methyl isothiocyanate (0.73 g.) using the conditions described in Example 132 afforded N-methyl)-N-[3-(4-methyl-2-oxazolyl)thiopropyl]thiourea (1.0 g.). m.p. 73°-74° (from ethanol-ether-n-hexane).
출처 및 근거
- ORD 기록
- ord-62fa46014e2640698d84a9d45967b214
- 출처 데이터셋
- uspto-grants-1979_01
- 특허 번호
- US04137234
연결된 노트
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