Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Anhydride → Citronellyl Acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | Citronellol | HCID 8842 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | Citronellyl Acetate | HCID 9017 | — |
반응 단계
100 Grams of 3,7-dimethyloct-6-en-1-ol is dissolved in 150 ml. of pyridine and 100 ml. of acetic anhydride and left at room temperature for about 48 hours. Then the mixture is extracted with ether and the ethereal extracts washed with water, 10% aqueous HCl and brine to yield 1-acetoxy-3,7-dimethyloct-6-ene which is purified by distillation.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04137273 |
| 출처 데이터셋 | uspto-grants-1979_01 |
| ORD ID | ord-bd39ca3e5fdc410baafd6f53f8e929f7 |
| 출처 메모 | uspto-grants-1979_01 |