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(5-Methylpyrimidin-2-yl)methanol → 5-Methylpyrimidine-2-carbaldehyde

HRID 2164994
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반응식

HRID 2164994 반응식
[OH:1][CH2:2][C:3]1[N:8]=[CH:7][C:6]([CH3:9])=[CH:5][N:4]=1>[O-2].[O-2].[Mn+4].C(Cl)(Cl)Cl>[CH3:9][C:6]1[CH:5]=[N:4][C:3]([CH:2]=[O:1])=[N:8][CH:7]=1
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참가 물질

4

반응물 1

HCID 23043337(5-Methylpyrimidin-2-yl)methanol

생성물 1

HCID 230433365-Methylpyrimidine-2-carbaldehyde

시약·촉매·용매 2

HCID 178418406HCID 178418406, 화합물촉매HCID 6212Chloroform용매

실험 절차

5-Methylpyrimidine-2-carboxaldehyde was prepared from 2-hydroxymethyl-5-methylpyrimidine by oxidation with excess manganese dioxide in boiling chloroform. The product was obtained as colourless crystals and was characterized by proton nuclear magnetic resonance spectroscopy. Proton nuclear magnetic resonance spectrum (CDCl3 ; δ in ppm): 2.44 (3H,s); 8.80 (2H,s); 10.06 (1H,s).

후처리

  1. customThe product was obtained as colourless crystals

출처 및 근거

ORD 기록
ord-2bdf565a13fb4b56a4133264da693543
출처 데이터셋
uspto-grants-1990_07
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04938793

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